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The aim of this investigation is to find the functional group by carrying out simple chemical tests and, later, identify the organic compound by using the spectra.

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Introduction

Identification of an Organic Unknown Said Q. I am given an investigation which I have to plan myself; it is about an unknown organic compound that is either an alcohol, aldehyde, ketone, carboxylic acid, ester or phenol. I have to suggest a series of simple chemical tests, which could be done in test tubes, to distinguish the functional group of this organic compound. I am going to be observing any change of colour, formation of precipitate or the evolution of gas when adding certain chemicals to this compound. The aim of this investigation is to find the functional group by carrying out simple chemical tests and, later, identify the organic compound by using the spectra. Chemicals and Apparatus * 10 * test tubes * measuring cylinder (5 cm3) * pipette * Bunsen burner * Splint * Gas syringe * Unknown organic compound * Brady's reagent * Bromine water * Sodium metal * Tollen's reagent * Calcium Carbonate * Limewater Safety Plan Read the method carefully and understand it before attempting on carrying out any experiment. ...read more.

Middle

So skip to Test 2.A. Test 1.B * To distinguish the carbonyl compound, measure 3 cm3 of the carbonyl compound in a measuring cylinder. * Pour this into a new test tube * Add 3-6 drops of Tollen's reagent (a solution of silver nitrate in aqueous ammonia) to the test tube. * If a silver mirror forms around the inside of the test tube, the compound is proved to be an aldehyde. However if no reaction occurs, it is a ketone. Test 2.A * Measure 3 cm3 of the unknown into a measuring cylinder. * Pour this into new a test tube. * Throw a pinch of Sodium metal to the unknown. * If gas is liberated, quickly light a splint and place it over the test tube. * If you hear a popping sound, this confirms that the gas is in fact Hydrogen and the unknown compound is either a phenol, alcohol or a carboxylic acid. ...read more.

Conclusion

* The gas should collect in the gas syringe. When gas stops evolving, bubble the gas into 5 cm3 of limewater. * If the limewater goes milky in colour, this proves that the gas is Carbon Dioxide and that the unknown is a carboxylic acid. * If no reaction occurs, then the unknown is confirmed to be an alcohol. Fair test Doing a fair test is completely essential for achieving accurate and reliable results which would take a large part in the conclusion at the end, and also for avoiding errors and anomalous results. I will make sure that this happens by many ways, by choosing: 1. Relevant and accurate equipment with very small percentage errors. 2. Washing and drying up the equipment thoroughly after each experiment ensuring that they are contamination-free. 3. Taking measurements carefully as specified by the method. 4. keeping a straight line of sight when reading measurements of solution in the measuring cylinder 5. Always read the bottom of the meniscus of any solution when taking measurements. ...read more.

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