• Join over 1.2 million students every month
  • Accelerate your learning by 29%
  • Unlimited access from just £6.99 per month

Testing unknown solutions.

Extracts from this document...


Chemistry Practical Test (Part A): Planning Exercise Testing unknown solutions Introduction In this practical investigation, I have to devise a logical sequence of chemical reactions to find out which unknown chemical goes with which name. I then have to outline a titration procedure for working out the exact concentration of aqueous nitric acid using aqueous sodium carbonate, concentration of 0.500 mol dm�� Precautions - Health and Safety * Wear safety glasses * Handle all chemicals with care * Wash hands before and after handling and chemicals * Have an eye wash available. Equipment Test tubes, Small pipette, Calcium carbonate (marble chips), Dilute hydrochloric acid, Silver nitrate, Nitric acid, Aqueous ammonia solution, Limewater, Delivery tube and stopper, Bunsen burner, Safety mat, Test tube holder Procedure (1) ...read more.


(3) Positive test for acids: Acid + carbonate carbon dioxide + water + salt * If both of the two unknown solutions left show a positive result, they are both acids, so I only need to work out either which is the nitric or the ethanoic acid, because the last solution would be the other acid. (4) Test for ethanoic acid: Esterification - if solution is ethanoic acid, it smells like pears. * Heat gently, allow to cool, smell cautiously Alcohol + carboxylic acid ester + water Danger - adding sulphuric acid to a dilute solution means that it could react with the water - could be explosive Risk assessment of Nitric acid * Corrosive * Oxidizing agent * Dangerous with ethanoic acid - if comes ...read more.


* Work out mean titre (for calculation = X) Calculation Solution A - nitric acid, volume - 25.0cm�, concentration - ? Solution B - sodium carbonate, volume - X, concentration - 0.500 mol dm�� 1000cm� of solution B = 0.5 mols NaCO3 In Xcm� NaCO3 there are: 0.5X / 1000 mol From equation: NaCO3 + HNO3 1 mol NaCO3 reacts with 1 mol HNO3 Mols HNO3 present in 1000cm� = (0.5X /1000) x 1000 25 = 0.5X � 25 The concentration of the nitric acid solution is therefore 0.5X � 25 mol.dm�� Fair test, precise and reliable data > Will repeat all experiments 3 times > All experiments - room temperature > Will use accurate equipment, e.g. calibrated pipette filler > Will compare data against specimen data to check reliability. Helen Spencer, candidate number: 9326, centre number: 55245 ...read more.

The above preview is unformatted text

This student written piece of work is one of many that can be found in our GCSE Aqueous Chemistry section.

Found what you're looking for?

  • Start learning 29% faster today
  • 150,000+ documents available
  • Just £6.99 a month

Not the one? Search for your essay title...
  • Join over 1.2 million students every month
  • Accelerate your learning by 29%
  • Unlimited access from just £6.99 per month

See related essaysSee related essays

Related GCSE Aqueous Chemistry essays

  1. Acidic Solutions.

    Using the funnel, I will rinse the burette with sulphuric acid (rinsing and filling the tip) and fill it with same solution. I will record the initial burette reading as trial. 2. Using pipette filler, I will rinse the pipette with some solution of sodium carbonate and carefully transfer 25.0cm of the solution into a clean 250cm conical flask.

  2. Titrating Sodium hydroxide with an unknown molarity, against hydrochloric acid to find its' molarity.

    However, I counted these types of figures as negligible. Later, the chemistry technician, who made up the sulphuric acid, was asked what the molarity of the sulphuric acid that was used within the titration was. It was 0.10moldm-3. Evaluation To evaluate this experiment where I titrated a standard solution of sodium carbonate against sulphuric acid of an unknown concentration,

  1. Identification of an Organic Unknown.

    The dilute acid provides both the acid catalyst and water. Repeat test three to check for presence of carboxylic acid. OR Esters have a distinct fruity smell. So you have to heat the organic unknown by using a Bunsen burner and a fruity smell will be present.

  2. Lipid Identification and Chromatography

    The result will be that the further up the paper a solute moves, the more soluble it is in the solvent, whereas the less soluble a solute is in that particular solvent, the lower up the paper it will move.

  • Over 160,000 pieces
    of student written work
  • Annotated by
    experienced teachers
  • Ideas and feedback to
    improve your own work