Titration Lab Report
CHEMISTRY LAB Titration Curves of Strong and Weak Acids and Bases Processing the Data: Questions: . Examine the time data for each of the Trials 1-4. In which trial(s) did the indicator change color at about the same time as the large increase in pH occurred at the equivalence point? In which trial(s) was there a significant difference in these two times? In all the 4 trials, the time taken for color change and the time taken for a large increase in pH was the same, leaving no significant difference between the two values. 2. Phenolphthalein changes from clear to red at a pH value of about 9. According to your results, with which combination(s) of strong or weak acids and bases can phenolphthalein be used to determine the equivalence point? The combination of a Strong Acid and Base will give us the equivalence point: there will be a color change of phenolphthalein at pH 9. It is also observed that the reaction between a Weak Acid and Strong Base can be used to obtain a pH of 9. 3. On each of the four printed graphs, draw a horizontal line from a pH value of 9 on the vertical axis to its intersection with the titration curve. In which trial(s) does this line intersect the nearly vertical region of the curve? In which trial(s) does this line miss the nearly vertical region of the curve? For Trials 1 and 3, the horizontal line from pH 9 intersects the S curve. For
Experiment to determine the ethanol content of wine
Experiment to Determine Ethanol Content of Wine The purpose of this experiment is to determine the ethanol content of each of the wines and compare the value determined to the value quoted on the label. These results can then be used to conclude which region is more accurate in quoting the value of the ethanol content of the wine. This experiment takes advantage of the fact that ethanol is less dense than water in solution. The density of ethanol at 20°C is 0.789 g/cm3 while the density of water at the same temperature is 0.998 g/cm3. It then follows that different solutions of ethanol and water will have different densities also, because the relative volume of ethanol increases and water decreases so the density of higher percentage ethanol solutions will be less than the density of lower percentage ethanol solutions. This occurs because water molecules are much smaller than ethanol molecule, meaning more water molecules can "pack" into a smaller volume than ethanol molecules, meaning there is more mass per unit volume of water compared to ethanol, meaning it has a higher density. In this experiment, solutions of ethanol in water were made up, going from 0% to 20%. These were then weighed, and the density of the ethanol was calculated. From this, a graph of percentage ethanol solution against density was made. This graphs later compared to the density of the wine, so
Preparation of propanone from propan-2-ol
Date: 11/10/2011 Exp. No.: 23 Title: Preparation of propanone from propan-2-ol Aim: The aim of this experiment is to prepare propanone by oxidizing propan-2-ol with acidified potassium dichromate solution. Introduction: Ketones and aldehydes are important series in preparation of other compounds and they are commonly prepared by oxidizing alcohol which is done in this experiment. The experiment is an oxidation reaction where a secondary alcohol (propan-2-ol) is oxidized by acidified potassium dichromate. The reaction does not need to be heated but should be placed in an iced water bath as the reaction is highly exothermic. The product is propanone and no catalyst is needed for the reaction. The propanone is serparated from the reaction mixture by simple distillation and is purified using anhydrous cacium chloride. The equation of this reaction is as follow: Chromic acid is produced in situ by adding potassium dichromate (VI) with sulphuric acid and water. K2Cr2O7 + H2O + 2H2SO4 ? 2 H2CrO4 + 2 NaHSO4 The term chromic acid is usually used for a mixture made by adding concentrated sulfuric acid to a dichromate, which may contain a variety of compounds, including solid chromium trioxide. Chromic acid features chromium in an oxidation state of +6. It is a strong and corrosive oxidising agent. Apparatus and chemicals: Apparatus: Quick-fit distillation setup,
The Development of the Periodic Table of the Elements
The Development of the Periodic Table of the Elements The periodic table is defined as the most common arrangement of the periodic system. This is the classification of chemical elements into periods (corresponding to the filling of successive electron shells) and groups (corresponding to the number of valence electrons) and describes the modern version that is used today. However, this was not always how it was structured and described - like the atom, the Periodic Table has been developed over time due to the contributions of a number of scientists (and is still developing even today). Long before the development of the modern Periodic Table, ancient philosophers such as Aristotle believed the world to be made up of four distinct elements: earth, water, air and fire. Although this is not true, they were thinking along the right lines as these are examples of the states of matter solids, liquids, gases and plasma. The first significant contribution towards the modern Periodic Table was made by the French chemist Lavoisier in 1789, who with his wife compiled the first modern chemical textbook named Traite Elementaire de Chimie (Elementary Treatise of Chemistry), which included a list of the known elements at the time. An advantage of Lavoisier's work is that he distinguished between metals and non-metals but a disadvantage was that he included some compounds and mixtures
Chemistry Module 1 revision notes - salts and redox reactions
Chemistry Module 1 Salts - A salt is an ionic compound with the following features: The positive ion or cation in a salt in a salt is usually a metal ion or an ammonium ion NH4 The negative ion or anion in a salt is derived from an acid Formation of Salts: Salts can be produced by neutralising acids with: - Carbonates - Bases - Alkalis Salts from bases: Acids react with bases to form a salt and water Salts from Carbonates: Acids react with carbonates to form a salt, CO2 and water Salts from alkalis: Acids react with alkalis to form a salt and water Salts from metals: Salts can be formed from the reaction of reactive metals with acids. There are known as redox reactions. Ammonia salts and fertilises: - Ammonia salts are used as artificial fertilisers - Ammonia salts are formed when acids are neutralised by aqueous ammonia Water of crystallisation -Water of crystallisation refers to water molecules that form an essential part of the crystalline structure of a compound. Often the compound cannot be crystallised if water molecules are not present. -The empirical formula of a hydrated compound is written in a unique way: -The empirical formula of the compound is separated from the water of crystallisation by a dot. - The relative number of water molecules of crystallisation is shown after a dot. Oxidation number: in a chemical formula each atom has an
Write an essay on electrode potentials.
F7 Essay Writing (Electrode Potentials) Q. Write an essay on electrode potentials. Outlines: (I) What are electrode potentials? (a) associated with equilibria of redox systems (half cells): e.g. metal / metal ion system ; non-metal / ion system ; ion / ion system; (b) reactivity, tendency for reduction to occur (losing electrons) and potential difference; (c) the potential difference of a half cell cannot be measured alone, but a relative value could be measured with another reference half cell / reference electrode; (d) a standard hydrogen electrode [SHE] (in which the emf is defined as zero) is used as the reference electrode; (II) How are electrode potentials measured? (a) concentration, temperature and pressure affect the emf of SHE, and the standard electrode potentials are obtained under conditions of 298K, 1 atm and conc. of 1M. (b) set up a cell with SHE and a salt bridge of electrolyte (e.g. KNO3); (c) a potentiometer is used to measure the cell emf (maximum potential difference), and the sign of cell emf = polarity of the right hand electrode. (III) How are electrode potentials used? / Application of electrode potentials? (a) calculation of cell emf ; (b) prediction of reaction feasibility and limitations. ~ Sample Essay ~ An electrode potential is the difference in an potential between an electrode and its surrounding electrolyte. It is
Experiment to Determine Acidities of Wine. The purpose of this experiment is to determine the total and volatile acidities of each of the wines and compare them.
Experiment to Determine Acidities of Wine The purpose of this experiment is to determine the total and volatile acidities of each of the wines and compare them. Acidity is a major contributor to the taste of wines. This is especially important in white wines, because there are very little tannins found in it, so acidity can affect the taste of the wine much more than in red wines. In this experiment, 0.1M Sodium Hydroxide solution is needed for titrations. Because this is not a standard solution, it is first standardised using oxalic acid. In order to calculate the total acidity of the wine, a titration with 0.1M sodium hydroxide is carried out with a pH meter. The pH of the wine and sodium hydroxide solution is measured when a certain volume of NaOH is added each time, and a titration curve of volume against pH is plotted. The volume for the solution to reach a pH of 8.2 is recorded. This is because NaOH is a strong alkali and wine is a weak acid, so the pH lies more to the side of the alkali. A pH of 8.2 as the equivalence point is a value agreed on by winemakers. In order to calculate the total acidity of the wine, a representative acid must be used. This must be chosen because wine contains multiple different acids, which require different moles of NaOH to neutralise them. Tartaric acid was chosen as the representative acid for the wine, because it is thought to
Revision Notes. Substances Manufactured for use in Industries. Chemicals, alloys and polymers.
.1 Manufacture of Sulphuric Acid Uses of Sulphuric Acid Sulphuric Acid, H2SO4, has many uses in our daily life. A few examples are: (a) Manufacture of fertilisers such as ammonium sulphate, (NH4) 2SO4 (b) Manufacture of electrolyte in lead-acid accumulators (c) Manufacture of soaps and detergents (d) Manufacture of pesticides (insecticide) (e) Manufacture of plastic items such as rayon and nylon (f) Manufacture of paints Manufacture of Sulphuric Acid in industry . Sulphuric acid, H2SO4, is manufactured in industry through the Contact Process. 2. The manufacturing of sulphuric acid, H2SO4, in industry involves three stages. Stage Aim Stage 1 Sulphur dioxide, SO2, gas can be produced by burning sulphur in air. S + O2 SO2 To produce sulphur dioxide, SO2, gas Stage 2 The gas mixture of sulphur dioxide and oxygen is passed over vanadium(V) oxide, V2O5 (catalyst) at a temperature of 450-500 ºC and under pressure of 1 atmosphere. 2SO2 + O2 2SO3 To produce sulphur trioxide, SO3 gas Stage 3 Sulphur trioxide, SO3, gas is dissolved in concentrated sulphuric acid, H2SO4 to form oleum, H2S2O7. SO3 + H2SO4 H2S2O7 Water is then added to the oleum, H2S2O7 to dilute it to produce sulphuric acid, H2SO4. H2S2O7 + H2O 2H2SO4 To produce sulphuric acid, H2SO4 The three stages involved in the Contact process Environmental
Experiment investigating hydrogen bonding in different chemicals.
Tsuen Wan Public Ho Chuen Yiu Memorial College Form 6 Chemistry Practical Experiment 8: Hydrogen Bonding Date of experiment: 27-1-2011 Objective: A. To discover the existence of hydrogen bonds between ethanol molecules B. To measure the strength of hydrogen bond formed between ethanol molecules C. To investigate the formation of hydrogen bonds between molecules of ethyl ethanoate and trichloromethane D. To measure the strength of hydrogen bonds formed between molecules of ethyl ethanoate and trichloromethane Introduction: A hydrogen bond is the attractive interaction of a hydrogen atom with an electronegative atom, such as nitrogen, oxygen or fluorine, that comes from another molecule or chemical group. The hydrogen must be covalently bonded to another electronegative atom to create the bond. These bonds can occur between molecules, or within different parts of a single molecule. The hydrogen bond (5 to 30 kJ/mol) is stronger than a van der Waals interaction, but weaker than covalent or ionic bonds. This type of bond occurs in both inorganic molecules such as water and organic molecules such as DNA. Intermolecular hydrogen bonding is responsible for the high boiling point of water (100 °C) compared to the other group 16 hydrides that have no hydrogen bonds. Intramolecular hydrogen bonding is partly responsible for the secondary, tertiary, and quaternary structures
Acid-Base titration by double indicator method
Date: 01/12/2010 Objective To determine the proportions of sodium carbonate and sodium hydroxide in a mixture solution using double indicator method. Procedures . 25 cm3 of the mixture solution was pipetted into a conical flask. 2. Two drops of phenolphthalein indicator were added into the conical flask. 3. The mixture solution was titrated with the given standard hydrochloric acid(0.098M). 4. The mixture was titrated to the end-point. 5. At the end point, the pink colour of phenolphthalein indicator was just discharged. 6. The burette reading (x) was recorded. 7. Two drops of methyl orange and a further quantity of acid were added 8. The mixture was titrated to the end-point. 9. At the end point ,the yellow colour of the methyl orange changed to orange. 0. The reading of that further quantity of acid (y) was recorded. 1. The steps above were repeated 3 times. Results: Volume of piptte used: 25 cm3 The concentration of the hydrochloric acid used: 0.098M x Trial 2 3 Final burette reading / cm3 2.40 31.80 29.40 2.70 Initial burette reading / cm3 0.10 9.50 7.20 0.30 Volume of acid used(x) / cm3 2.30 2.30 2.20 2.40 Mean value of x= (12.30+12.20+12.40)/3 =12.30 cm3 y Trial 2 3 Final burette reading / cm3 9.50 38.80 36.60 9.80 Initial burette reading / cm3 2.40 31.80 29.40 2.70 Volume of acid used(x) / cm3 7.10 7.00
