Design
Purpose: To determine the empirical formula of Magnesium Oxide
Independent Variable: amount of oxygen available
Dependent Variable: amount of magnesium oxide produced
Controlled Variables:
Heat of the flame, height of the flame, room temperature, mass of magnesium strip, and the same electronic balance were some of the controlled variables in this experiment. For all the trials that were conducted, the gas valve and the needle valve were not altered which kept the flame consistent- intensity and height. Since the whole experiment was completed during one period and in the same room the room temperature remained the same. 10cm±0.1cm of magnesium strip was measured for each trial and the mass each time was around 2.0g±0.1g. The same electronic balance was used to minimize the error.
Materials
Procedure
- Safety First! Put on goggles
- Using a balance, determine the mass of a clean, dry porcelain crucible and lid
- Clean the surface of a 10 cm±0.01cm strip of magnesium ribbon with steel wool. Loosely coil the magnesium ribbon and place it in the crucible
- Determine the mass of the crucible, lid and magnesium ribbon.
- Place the crucible securely on a clay triangle. Set the lid slightly off-centre on the crucible to allow air to enter but prevent the magnesium oxide from escaping
- Heat the bottom of the crucible with a gentle flame
- Gradually increase the flame intensity until all the magnesium turns into a white powder. Remove the burner and lift the lid after you observe no more smoke coming from the burner. Continue heating until the crucible contains only white powder
- When you no longer have any magnesium ribbon, turn off the burner and allow the crucible, lid and contents to cool
- Measure the mass of the crucible, lid and contents.
- Clean up the work area
- Find the average mass of oxygen in the experiment
- Find the average mass of magnesium in the experiment
- Find the molar mass of O and Mg
- Calculate the moles of O present magnesium oxide
- Calculate the moles of Mg present magnesium oxide
- Determine the mole ratio
- Determine the average mass of the magnesium oxide
- Determine the percent composition of magnesium oxide